HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one → (3-Nitro-phenyl)-(4-pyridin-3-yl-pyrimidin-2-yl)-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one | HCID 567033 | — |
| Edukt | 3-Nitrophenylguanidine Nitrate | HCID 178512513 | — |
| Produkt | (3-Nitro-phenyl)-(4-pyridin-3-yl-pyrimidin-2-yl)-amine | HCID 9860872 | 69,7% |
Reaktionsschritte
3-Nitrophenyl-guanidine nitrate (28 g, 0.12 mol) and 3-dimethylamino-1-(3-pyridyl)-2-propen-1-one (16.9 g, 0.09 mol) were reacted according to the same procedure as Step 1.3 of Preparation 1 to give N-(3-nitrophenyl)-4-(3-pyridyl)-2-pyrimidine-amine (18.4 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07595323B2 |
| Quelldatensatz | uspto-grants-2009_09 |
| ORD ID | ord-18ee62cb361345d79978b33f89b667b2 |
| Quellennotiz | uspto-grants-2009_09 |