HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
L-Valinol → N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | L-Valinol | HCID 640993 | — |
| Edukt | 1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid | HCID 57672890 | — |
| Produkt | N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol | HCID 24875907 | — |
Reaktionsschritte
2.00 g (7.48 mmol) of 1-[[(2-furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid was used instead of 2-benzothiophenecarboxylic acid, and 772 mg (7.48 mmol) of L-valinol was used instead of 1-aminocyclohexanecarboxylic acid phenylmethyl ester in the process according to Reference Example 197 to obtain 2.67 g (quantitative) of the title compound and 2.64 g (quantitative) of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08829209B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-2f1ffac19e114f4d97b2ad5ddb4635e3 |
| Quellennotiz | uspto-grants-2014_09 |