HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Bromobutane → 3-sec-Butyl-1H-indol-6-ylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Bromobutane | HCID 6554 | — |
| Edukt | 6-Nitro-1H-indole | HCID 78502 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 3-sec-Butyl-1H-indol-6-ylamine | HCID 57470200 | — |
Reaktionsschritte
3-sec-Butyl-1H-indol-6-ylamine (B-14) was synthesized following the general scheme above starting from 6-nitroindole and 2-bromobutane. Overall yield (20%). HPLC ret. time 2.32 min, 10-99% CH3CN, 5 min run; ESI-MS 189.5 m/z (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08829204B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-9e49ae8cd83446ca958e78fb7ba17cdc |
| Quellennotiz | uspto-grants-2014_09 |