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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 742080Erstellt: 24. Oktober 2026

alpha-Hydroxyacetophenone → Flavonol

https://huagongshe.com/de/reaction/742080

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Eduktalpha-HydroxyacetophenoneHCID 68490—
Edukt(1,1'-Biphenyl)-4-carboxaldehydeHCID 76689—
LösungsmittelEthanolHCID 702—
LösungsmittelSodium HydroxideHCID 14798—
ProduktFlavonolHCID 11349—

Reaktionsschritte

180 mg of 4'-vinyl, 4-biphenyl aldehyde was mixed with 0.3 ml of 2-hydroxyacetophenone in 30 ml of ethanol. In a separate flask, 2.0 gms of NaOH was dissolved in 10 ml of aq. ethyl alcohol (50%). An NaOH solution was slowly added to the aldehyde solution. The resulting solution slowly changed its color from green to yellow to dark red. The rest of the reaction was carried out according to the method described in Example 1(b) above, producing 4'styryl, 3-hydroxyflavone.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05552551
Quelldatensatzuspto-grants-1996_09
ORD IDord-21ed05cb9ada411cb768795976d60d3f
Quellennotizuspto-grants-1996_09