HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
alpha-Hydroxyacetophenone → Flavonol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | alpha-Hydroxyacetophenone | HCID 68490 | — |
| Edukt | (1,1'-Biphenyl)-4-carboxaldehyde | HCID 76689 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Lösungsmittel | Sodium Hydroxide | HCID 14798 | — |
| Produkt | Flavonol | HCID 11349 | — |
Reaktionsschritte
180 mg of 4'-vinyl, 4-biphenyl aldehyde was mixed with 0.3 ml of 2-hydroxyacetophenone in 30 ml of ethanol. In a separate flask, 2.0 gms of NaOH was dissolved in 10 ml of aq. ethyl alcohol (50%). An NaOH solution was slowly added to the aldehyde solution. The resulting solution slowly changed its color from green to yellow to dark red. The rest of the reaction was carried out according to the method described in Example 1(b) above, producing 4'styryl, 3-hydroxyflavone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05552551 |
| Quelldatensatz | uspto-grants-1996_09 |
| ORD ID | ord-21ed05cb9ada411cb768795976d60d3f |
| Quellennotiz | uspto-grants-1996_09 |