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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 742225Erstellt: 24. Oktober 2026

Triethylamine → 4-Imidazolidinone, 3-(diphenylmethyl)-1-methyl-2-thioxo-

https://huagongshe.com/de/reaction/742225

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriethylamineHCID 8471—
EduktEthyl N-methylaminoacetate hydrochlorideHCID 171173—
EduktBenzhydryl isothiocyanateHCID 520742—
LösungsmittelChloroformHCID 6212—
Produkt4-Imidazolidinone, 3-(diphenylmethyl)-1-methyl-2-thioxo-HCID 11150625—

Reaktionsschritte

The title compound was prepared by the procedure described in Example 1 using 11.25 g of benzhydryl-isothiocyanate, 7.68 g of sarcosine ethyl ester hydrochloride, 12 g of triethyl amine, and 200 mL of chloroform. The title compound was obtained (7.40 g) as an off-white solid, m.p. 139°-141° C. Anal. Calcd. for C17H16N2O S: C, 68.89; H, 5.44; N, 9.45. Found: C, 68.92; H, 5.43; N, 9.58. Mass spectrum (El, M.+) m/z 296.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05554607
Quelldatensatzuspto-grants-1996_09
ORD IDord-bd0b8e661d7844e99bc0f045247d5240
Quellennotizuspto-grants-1996_09