Methyl carbazate → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Hydrazinocarbonylhydrazinecarboxylate

HRID 742621Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 742621
[C:1]([O:5][CH:6]1[CH2:11][C:10]([CH3:13])([CH3:12])[N:9]([O:14][CH3:15])[C:8]([CH3:17])([CH3:16])[CH2:7]1)(=[O:4])[NH:2][NH2:3].[C:18](OC)(=[O:21])[NH:19][NH2:20]>CO>[NH:19]([C:18]([NH:3][NH:2][C:1]([O:5][CH:6]1[CH2:7][C:8]([CH3:17])([CH3:16])[N:9]([O:14][CH3:15])[C:10]([CH3:12])([CH3:13])[CH2:11]1)=[O:4])=[O:21])[NH2:20]

Komponenten

4

Edukt 2

HCID 80519Methyl carbazateHCID 536527591-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

Produkt 1

HCID 542840721-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Hydrazinocarbonylhydrazinecarboxylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

The title compound is prepared by reacting the compound of Example 28 (1 mole) with methyl carbazate (1 mole) by refluxing the reaction mixture in methanol.

Quellen und Nachweise

ORD-Eintrag
ord-807ca6456c72435b8f5530f74d6af241
Quelldatensatz
uspto-grants-1996_09
Patentnummer
US05554754

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