HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoate → Benzoate maleate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoate | HCID 242 | — |
| Edukt | Maleic Acid | HCID 444266 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Benzoate maleate | HCID 68560292 | — |
Reaktionsschritte
In 3 mL of ethyl acetate was dissolved 0.25 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate, and 0.07 g of maleic acid was added thereto, after which the resulting mixture was heated to effect dissolution. The reaction mixture was cooled and the crystals precipitated were collected by filtration to obtain 0.15 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate maleate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087594B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-595bfc092f2a49439306456243cac199 |
| Quellennotiz | uspto-grants-2006_08 |