Hydrochloric Acid → Benzoic acid, 2-(aminosulfonyl)-, methyl ester
Reaktionsgleichung
Cl.[S:2]1([C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:6](=[O:7])[NH:5]1)(=[O:4])=[O:3].[CH3:14][OH:15]>>[CH3:14][O:15][C:6](=[O:7])[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=1[S:2](=[O:4])(=[O:3])[NH2:5]Komponenten
4
Versuchsvorschrift
An HCl stream is led under cooling into a suspension of 143.3 g (0.78 mol) in 600 ml absolute methanol until saturation. Subsequently the solution is refluxed yet two hours until the saccharine has gone completely into solution and the reaction has terminated.
Aufarbeitung
- customthe reaction has terminated
Quellen und Nachweise
- ORD-Eintrag
- ord-7682b66929384626b8eedbdba4fb52da
- Quelldatensatz
- uspto-grants-1986_07
- Patentnummer
- US04601746
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