Hydrochloric Acid → Benzoic acid, 2-(aminosulfonyl)-, methyl ester

HRID 745889

Reaktionsgleichung

Reaktionsgleichung von HRID 745889
Cl.[S:2]1([C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:6](=[O:7])[NH:5]1)(=[O:4])=[O:3].[CH3:14][OH:15]>>[CH3:14][O:15][C:6](=[O:7])[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=1[S:2](=[O:4])(=[O:3])[NH2:5]

Komponenten

4

Edukt 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 5143Saccharin

Produkt 1

HCID 42546Benzoic acid, 2-(aminosulfonyl)-, methyl ester

Versuchsvorschrift

An HCl stream is led under cooling into a suspension of 143.3 g (0.78 mol) in 600 ml absolute methanol until saturation. Subsequently the solution is refluxed yet two hours until the saccharine has gone completely into solution and the reaction has terminated.

Aufarbeitung

  1. customthe reaction has terminated

Quellen und Nachweise

ORD-Eintrag
ord-7682b66929384626b8eedbdba4fb52da
Quelldatensatz
uspto-grants-1986_07
Patentnummer
US04601746

Verknüpfte Notizen

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