HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → 1-Amino-1-(2,2,5,5-tetramethyl-1-cyclopentyl)ethenylcyclopropane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | N-Boc-1-amino-1-(2,2,5,5-tetramethyl-1-cyclopentyl)ethenylcyclopropane | HCID 70445455 | — |
| Lösungsmittel | Trifluoroacetic acid | HCID 6422 | — |
| Produkt | 1-Amino-1-(2,2,5,5-tetramethyl-1-cyclopentyl)ethenylcyclopropane | HCID 20164442 | — |
Reaktionsschritte
N-Boc-1-amino-1-(2,2,5,5-tetramethyl-1-cyclopentyl)ethenylcyclopropane is dissolved in trifluoroacetic acid and the solution is stirred overnight. Water is added and the mixture is made basic with 20% KOH. The mixture is extracted with ether, and the organic layer is dried over Na2SO4 and is evaporated to yield 1-amino-1-(2,2,5,5-tetramethyl-1-cyclopentyl)ethenylcyclopropane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04603012 |
| Quelldatensatz | uspto-grants-1986_07 |
| ORD ID | ord-fa1ab37073b8466690f34c54835671c3 |
| Quellennotiz | uspto-grants-1986_07 |