Hydrochloric Acid → HCID 68833752, Verbindung

HRID 747688Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 747688
[CH3:1][N:2]([CH2:9][C:10]([O:12]CC)=[O:11])[C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1.[ClH:15]>O1CCOCC1>[ClH:15].[CH3:1][N:2]([CH2:9][C:10]([OH:12])=[O:11])[C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 62006965HCID 62006965, Verbindung

Produkt 1

HCID 68833752HCID 68833752, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 312751,4-DioxaneLösungsmittel

Reaktionsbedingungen

Temperatur
95 °C

Versuchsvorschrift

1.28 g (6.60 mmol) of ethyl [N-methyl-N-(pyridine-4-yl)amino]acetate was stirred in 30 ml of dioxane. 26 ml of 1 N hydrochloric acid was added to the resultant mixture, and they were stirred at 95° C. for 20 hours. The solvent was evaporated under reduced pressure to obtain the title compound.

Aufarbeitung

  1. customThe solvent was evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-d50aa3187b334e6f9906fff4cd7c8c1d
Quelldatensatz
uspto-grants-2008_07
Patentnummer
US07396844B1

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