Ethanol → Ethyl sulfoacetate

HRID 747777

Reaktionsgleichung

[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH2:9](O)[CH3:10]>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

Komponenten

Edukt 2

HCID 702Ethanol

HCID 31257Sulfoacetic acid

Produkt 1

HCID 12216623Ethyl sulfoacetate

Reaktionsbedingungen

Temperatur: 80 °C

Versuchsvorschrift

2.21 g (15.8 mmol) of sulfoacetic acid was suspended in 30 ml of ethanol, and the suspension was heated at 80° C. under reflux for 5 hours. The solvent was distilled off to obtain the title compound.

Aufarbeitung

temperatureunder reflux for 5 hours
distillationThe solvent was distilled off

Quellen und Nachweise

ORD-Eintrag: ord-7c0ee0c177f14bd0af3e41d8c0c28fe5
Quelldatensatz: uspto-grants-2008_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07396844B1

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