HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium hydride → HCID 22235051, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 1-(Bromomethyl)-4-(propan-2-yl)benzene | HCID 47719 | — |
| Edukt | 2-(3,3,3-Trifluoropropyl)malononitrile | HCID 22185761 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | HCID 22235051 | HCID 22235051 | 85% |
Reaktionsschritte
Using 0.21 g of 4-isopropylbenzyl bromide, 3 ml of N,N-dimethylformamide, 0.05 g of sodium hydride (60% in oil), and 0.17 g of (3,3,3-trifluoropropyl)malononitrile, and according to the process described in the Production Example 26, there was obtained 0.24 g of 2-(4-isopropylbenzyl)-2-(3,3,3-trifluoropropyl)malononitrile (the present compound (35)).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07402691B2 |
| Quelldatensatz | uspto-grants-2008_07 |
| ORD ID | ord-6550b84f378d454888d2a814ca801951 |
| Quellennotiz | uspto-grants-2008_07 |