HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tetrahydrofuran → 2-(2,4-Dichlorobenzyl)malononitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tetrahydrofuran | HCID 8028 | — |
| Edukt | 2,4-Dichlorobenzylidenemalononitrile | HCID 18089 | — |
| Edukt | Sodium borohydride | HCID 4311764 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2-(2,4-Dichlorobenzyl)malononitrile | HCID 2764143 | 69% |
Reaktionsschritte
Using 4.46 g of (2,4-dichlorobenzylidene)malononitrile, 20 ml of tetrahydrofuran, and a suspension of 0.19 g of sodium borohydride in 5 ml of ethanol, and according to the process described in Reference Production Example 8, there was obtained 3.10 g of (2,4-dichlorobenzyl)malononitrile (the intermediate (13)).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07402691B2 |
| Quelldatensatz | uspto-grants-2008_07 |
| ORD ID | ord-7b76ed23bc784220a158178cd72a30af |
| Quellennotiz | uspto-grants-2008_07 |