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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7508Erstellt: 24. Oktober 2026

Benzaldehyde → HCID 178419019, Verbindung

https://huagongshe.com/de/reaction/7508

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzaldehydeHCID 240—
EduktAcetyl chlorideHCID 6367—
EduktTert-Butyl isocyanideHCID 23577—
EduktAminopyrazineHCID 78747—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419019HCID 178419019—

Reaktionsschritte

Example 2 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrazine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-e0ba9380ec10483696e9cccc1e07c5c7
Quellennotizuspto-grants-2006_08