4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
Reaktionsgleichung
S(Cl)([Cl:3])=O.[CH2:5]([O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18](O)=[O:19])=[CH:16][CH:15]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>>[CH2:5]([O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18]([Cl:3])=[O:19])=[CH:16][CH:15]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]Komponenten
3
Versuchsvorschrift
A large excess of thionyl chloride was added to 10 g of the p-octyloxybenzoic acid prepared in (1), and the mixture was refluxed for 5 hours. Excessive thionyl chloride was distilled off to give a crude end compound.
Aufarbeitung
- temperaturethe mixture was refluxed for 5 hours
- distillationExcessive thionyl chloride was distilled off
- customto give a crude end compound
Quellen und Nachweise
- ORD-Eintrag
- ord-89aff4b1c18042e4bbb1f88ebba96f86
- Quelldatensatz
- uspto-grants-1998_03
- Patentnummer
- US05723069
Notizen zur Reaktion
Wird geladen…