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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7512Erstellt: 23. Oktober 2026

Benzaldehyde → HCID 178418850, Verbindung

https://huagongshe.com/de/reaction/7512

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzaldehydeHCID 240—
EduktAcetyl chlorideHCID 6367—
Edukt2-AminopyrimidineHCID 7978—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178418850HCID 178418850—

Reaktionsschritte

Example 6 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-c75393935092495082753744d346cd4a
Quellennotizuspto-grants-2006_08