HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzaldehyde → HCID 178418850, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzaldehyde | HCID 240 | — |
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | 2-Aminopyrimidine | HCID 7978 | — |
| Edukt | Cyclohexyl isocyanide | HCID 79129 | — |
| Lösungsmittel | Perchloric Acid | HCID 24247 | — |
| Produkt | HCID 178418850 | HCID 178418850 | — |
Reaktionsschritte
Example 6 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087607B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-c75393935092495082753744d346cd4a |
| Quellennotiz | uspto-grants-2006_08 |