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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7513Erstellt: 23. Oktober 2026

Acetaldehyde → HCID 178418843, Verbindung

https://huagongshe.com/de/reaction/7513

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetaldehydeHCID 177—
EduktAcetyl chlorideHCID 6367—
EduktCyclohexyl isocyanideHCID 79129—
Edukt2-Amino-3-benzyloxypyridineHCID 90334—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178418843HCID 178418843—

Reaktionsschritte

Example 7 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-3-benzyloxypyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-efb2df06a3ae44799f8795ccf59d72ac
Quellennotizuspto-grants-2006_08