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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7516Erstellt: 23. Oktober 2026

Benzaldehyde → HCID 178418783, Verbindung

https://huagongshe.com/de/reaction/7516

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzaldehydeHCID 240—
Edukt2-AminopyridineHCID 10439—
EduktTert-Butyl isocyanideHCID 23577—
EduktCyclohexanecarbonyl chlorideHCID 75938—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178418783HCID 178418783—

Reaktionsschritte

Example 10 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process steps b) to d) by reacting the resultant reaction product with 0.4 mmol cyclohexylcarboxylic acid chloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-cb1d1f9e1bc94670a80cb99ed22a0e19
Quellennotizuspto-grants-2006_08