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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7517Erstellt: 24. Oktober 2026

Benzaldehyde → HCID 178419071, Verbindung

https://huagongshe.com/de/reaction/7517

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzaldehydeHCID 240—
EduktOctanoyl chlorideHCID 8124—
Edukt2-AminopyridineHCID 10439—
EduktTert-Butyl isocyanideHCID 23577—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419071HCID 178419071—

Reaktionsschritte

Example 11 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process steps b) to d) by reacting the resultant reaction product with 0.4 mmol heptylcarboxylic acid chloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-fed35cec3dc043e3b9de4b02712093a2
Quellennotizuspto-grants-2006_08