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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7524Erstellt: 24. Oktober 2026

Acetyl chloride → HCID 178419044, Verbindung

https://huagongshe.com/de/reaction/7524

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetyl chlorideHCID 6367—
Edukt2-PyridinecarboxaldehydeHCID 14273—
EduktAminopyrazineHCID 78747—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419044HCID 178419044—

Reaktionsschritte

Example 18 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrazine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) pyridine-2-carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-a7f6f74d3a9f43fa8b7eb8ec0624032a
Quellennotizuspto-grants-2006_08