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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7525Erstellt: 23. Oktober 2026

Acetyl chloride → HCID 178419033, Verbindung

https://huagongshe.com/de/reaction/7525

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetyl chlorideHCID 6367—
Edukt2-AminopyrimidineHCID 7978—
Edukt2-PyridinecarboxaldehydeHCID 14273—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419033HCID 178419033—

Reaktionsschritte

Example 19 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) pyridine-2-carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-1cc3531c804049d985d00a34b502b64b
Quellennotizuspto-grants-2006_08