HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetyl chloride → HCID 178419033, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | 2-Aminopyrimidine | HCID 7978 | — |
| Edukt | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Edukt | Cyclohexyl isocyanide | HCID 79129 | — |
| Lösungsmittel | Perchloric Acid | HCID 24247 | — |
| Produkt | HCID 178419033 | HCID 178419033 | — |
Reaktionsschritte
Example 19 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) pyridine-2-carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087607B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-1cc3531c804049d985d00a34b502b64b |
| Quellennotiz | uspto-grants-2006_08 |