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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7527Erstellt: 23. Oktober 2026

Acetyl chloride → HCID 178418949, Verbindung

https://huagongshe.com/de/reaction/7527

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetyl chlorideHCID 6367—
Edukt2-Amino-4,6-dimethyl pyrimidineHCID 13021—
Edukt2-PyridinecarboxaldehydeHCID 14273—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178418949HCID 178418949—

Reaktionsschritte

Example 21 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-4,6-dimethylpyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) pyridine-2-carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-368f336e81b8446b9e73adc393321be5
Quellennotizuspto-grants-2006_08