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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7528Erstellt: 24. Oktober 2026

2-Aminothiazole → HCID 178418835, Verbindung

https://huagongshe.com/de/reaction/7528

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-AminothiazoleHCID 2155—
EduktAcetyl chlorideHCID 6367—
Edukt2-PyridinecarboxaldehydeHCID 14273—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178418835HCID 178418835—

Reaktionsschritte

Example 22 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-aminothiazole (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) pyridine-2-carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-ae6a67ef2da04b86bbc2bf27489624ee
Quellennotizuspto-grants-2006_08