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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7529Erstellt: 24. Oktober 2026

Acetyl chloride → HCID 178418859, Verbindung

https://huagongshe.com/de/reaction/7529

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetyl chlorideHCID 6367—
Edukt2-AminopyridineHCID 10439—
EduktCyclohexanecarboxaldehydeHCID 16275—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178418859HCID 178418859—

Reaktionsschritte

Example 23 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) cyclohexane carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-d6b7304d14924773a356ec02ce0f21c6
Quellennotizuspto-grants-2006_08