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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7530Erstellt: 23. Oktober 2026

Acetaldehyde → HCID 178419014, Verbindung

https://huagongshe.com/de/reaction/7530

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetaldehydeHCID 177—
EduktAcetyl chlorideHCID 6367—
Edukt2-AminopyrimidineHCID 7978—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419014HCID 178419014—

Reaktionsschritte

Example 24 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-d0df49b2497040b5aed415ee76af723d
Quellennotizuspto-grants-2006_08