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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 7531Erstellt: 24. Oktober 2026

Acetaldehyde → HCID 178419096, Verbindung

https://huagongshe.com/de/reaction/7531

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetaldehydeHCID 177—
EduktAcetyl chlorideHCID 6367—
Edukt2,4-Diamino-6-chloropyrimidineHCID 67432—
EduktCyclohexyl isocyanideHCID 79129—
LösungsmittelPerchloric AcidHCID 24247—
ProduktHCID 178419096HCID 178419096—

Reaktionsschritte

Example 25 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2,6-diamino-4-chloro-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μL perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087607B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-d226efdb4de84acf86dab433a563b9d9
Quellennotizuspto-grants-2006_08