HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentanecarbonyl chloride → N-[1-(3-tert-butyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclopentanecarboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentanecarbonyl chloride | HCID 78284 | — |
| Edukt | 6-(1-Aminopropyl)-3-tert-butyl-1,2,4-triazin-5(4h)-one | HCID 135594090 | — |
| Produkt | N-[1-(3-tert-butyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclopentanecarboxamide | HCID 135752563 | — |
Reaktionsschritte
In analogy to the procedure for Example 36A, 110 mg (0.50 mmol) 6-(1-aminopropyl)-3-tert-butyl-1,2,4-triazin-5(4H)-one, 70 mg (0.50 mmol) cyclopentanecarbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087605B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-b46f015255f1488ebf4026b731b6fb22 |
| Quellennotiz | uspto-grants-2006_08 |