HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentanecarbonyl chloride → N-{1-[3-(4-methyl-1-naphthyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]propyl}cyclopentanecarboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentanecarbonyl chloride | HCID 78284 | — |
| Edukt | 6-(1-aminopropyl)-3-(4-methyl-1-naphthyl)-1,2,4-triazin-5(4H)-one | HCID 135752639 | — |
| Produkt | N-{1-[3-(4-methyl-1-naphthyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]propyl}cyclopentanecarboxamide | HCID 135752584 | — |
Reaktionsschritte
In analogy to the procedure for Example 36A, 600 mg (2.04 mmol) 6-(1-aminopropyl)-3-(4-methyl-1-naphthyl)-1,2,4-triazin-5(4H)-one, 270 mg (2.04 mmol) cyclopentanecarbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087605B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-3515f6f04b2e4e65bb53076e6c2d4d2c |
| Quellennotiz | uspto-grants-2006_08 |