HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → 2-Oxopyrrolidine-3-carboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Ethyl 2-oxopyrrolidine-1-carboxylate | HCID 234959 | — |
| Produkt | 2-Oxopyrrolidine-3-carboxylic acid | HCID 13474370 | — |
Reaktionsschritte
To 0.50 g (3.18 mmol) 2-oxo-pyrollidine-carboxylic acid ethyl ester in 10 mL EtOH are added 5 mL aq. NaOH (1M) solution. The reaction mixture is stirred at r.t. for 3 h. The EtOH is removed in vacuo and the residue is diluted with water and acidified with aq. HCl (2M) solution. The resulting precipitate is filtered and dried.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08835472B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-eb7275050f334e848da4cf494465570b |
| Quellennotiz | uspto-grants-2014_09 |