Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 76280Erstellt: 23. Oktober 2026

3-Oxocyclopentanecarboxylic acid → HCID 178441291, Verbindung

https://huagongshe.com/de/reaction/76280

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Oxocyclopentanecarboxylic acidHCID 227798—
Edukt2-tert-Butyl-4-butylisothiazol-5(2H)-imineHCID 66867228—
ProduktHCID 178441291HCID 178441291—

Reaktionsschritte

The product from Example 92B and 3-oxocyclopentanecarboxylic acid (Aldrich) were processed using the method described in Example 92C to afford the title compound. 1H NMR (DMSO-d6) δ 0.91 (t, J=7.5 Hz, 3H), 1.25-1.36 (m, 2H), 1.57 (s, 9H), 1.55-1.84 (m, 2H), 1.98-2.06 (m, 1H), 2.13-2.28 (m, 3H), 2.39-2.42 (m, 2H), 2.61-2.66 (m, 2H), 3.27-3.34 (m, 1H), 8.55 (s, 1H). MS (ESI+) m/z 323 (M+H)+. Anal. calcd. for C17H26N2O2S: C, 63.32; H, 8.13; N, 8.69. Found: C, 63.19; H, 8.07; N, 8.66.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08835475B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-6187a47ae84340b19d3a641f0e5b7e4c
Quellennotizuspto-grants-2014_09