HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chloroacetonitrile → 2-(2-Amino-2-oxoethoxy)-5-chlorobenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chloroacetonitrile | HCID 7856 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Benzoic acid, 5-chloro-2-hydroxy-, methyl ester | HCID 77684 | — |
| Produkt | 2-(2-Amino-2-oxoethoxy)-5-chlorobenzoic acid | HCID 8707311 | — |
Reaktionsschritte
Commercially available, methyl 5-chloro-2-hydroxybenzoate (Maybridge), potassium carbonate, 2-chloroacetonitrile (Aldrich) and sodium hydroxide were processed according to the method described for Example 130A to obtain the title compound. MS (ESI+) m/z 248 (M+H2O)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08835475B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-f9f72c43914943f5adde9c82ee6c9f48 |
| Quellennotiz | uspto-grants-2014_09 |