Reaktionsgleichung
[CH:1](=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[F:8][C:9]([F:15])([F:14])[C:10]([CH3:13])([NH2:12])[CH3:11].[C:16]([N:21]=[C:22]=[S:23])(=[O:20])[O:17][CH2:18][CH3:19].II>>[CH2:3]([C:2]1=[CH:1][N:12]([C:10]([CH3:13])([CH3:11])[C:9]([F:15])([F:14])[F:8])[S:23]/[C:22]/1=[N:21]\[C:16](=[O:20])[O:17][CH2:18][CH3:19])[CH2:4][CH2:5][CH3:6]Komponenten
5
Versuchsvorschrift
Commercially available hexanal (Aldrich), 1,1,1-trifluoro-2-methylpropan-2-amine (Chemcollect), O-ethyl carbonisothiocyanatidate (Aldrich) and iodine were processed using the method described in Example 110A to afford the title compound. MS (ESI+) m/z 339 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-2cd5d913d41e441eb5cc445ddd0aa78f
- Quelldatensatz
- uspto-grants-2014_09
- Patentnummer
- US08835475B2
Verknüpfte Notizen
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