HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 78488Erstellt: 24. Oktober 2026
Allyl bromide → 3-allyl-4,5-dimethylthiazol-2(3H)-imine hydrobromide
https://huagongshe.com/de/reaction/78488
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Allyl bromide | HCID 7841 | — |
| Edukt | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 3-allyl-4,5-dimethylthiazol-2(3H)-imine hydrobromide | HCID 68623542 | — |
Reaktionsschritte
A mixture of 4,5-dimethyl-1,3-thiazol-2-amine (1 g) and allylbromide (0.95 g) in toluene (5 mL) was heated to 85° C. for 12 hours, cooled, diluted with ether, filtered and the solvent was evaporated to afford crude product that was taken on to the next step without further characterization.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08841334B2 |
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| Quelldatensatz | uspto-grants-2014_09 |
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| ORD ID | ord-b550bf94e1dc44afbb8ef0c33f28bdba |
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| Quellennotiz | uspto-grants-2014_09 |
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