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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 78488Erstellt: 24. Oktober 2026

Allyl bromide → 3-allyl-4,5-dimethylthiazol-2(3H)-imine hydrobromide

https://huagongshe.com/de/reaction/78488

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAllyl bromideHCID 7841—
Edukt2-Amino-4,5-dimethyl-1,3-thiazoleHCID 73238—
LösungsmittelTolueneHCID 1140—
LösungsmittelDiethyl EtherHCID 3283—
Produkt3-allyl-4,5-dimethylthiazol-2(3H)-imine hydrobromideHCID 68623542—

Reaktionsbedingungen

Temperatur85 °C

Reaktionsschritte

A mixture of 4,5-dimethyl-1,3-thiazol-2-amine (1 g) and allylbromide (0.95 g) in toluene (5 mL) was heated to 85° C. for 12 hours, cooled, diluted with ether, filtered and the solvent was evaporated to afford crude product that was taken on to the next step without further characterization.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08841334B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-b550bf94e1dc44afbb8ef0c33f28bdba
Quellennotizuspto-grants-2014_09