HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
O-Methylhydroxylamine → N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | O-Methylhydroxylamine | HCID 4113 | — |
| Edukt | 3-[(2-Chloro-4-iodophenyl)amino]isonicotinic acid | HCID 57649651 | — |
| Produkt | N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide | HCID 11589486 | — |
Reaktionsschritte
N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.30 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.42 mmol of O-methyl-hydroxylamine. LC/MS [8.75 min; 404 (M+1)]
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08841459B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-97e83a8c3a8e47f1a98c2fc1460c4b20 |
| Quellennotiz | uspto-grants-2014_09 |