Imidazole → 1-[Bis(methylphenyl)methyl]imidazole

HRID 80324

Reaktionsgleichung

Reaktionsgleichung von HRID 80324
[C:1]1([C:7]2[CH:12]=[CH:11]N=C(CN3C=CN=C3)[C:8]=2[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:6]=[CH:5][CH:4]=CC=1.[CH3:25]C1C=CC(C(C2C=CC(C)=CC=2)O)=CC=1.S(Cl)(Cl)=O.[NH:45]1[CH:49]=[CH:48][N:47]=[CH:46]1>>[CH3:25][C:24]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[CH:8]([C:7]1[CH:1]=[CH:6][CH:5]=[CH:4][C:12]=1[CH3:11])[N:45]1[CH:49]=[CH:48][N:47]=[CH:46]1

Komponenten

5

Edukt 4

HCID 795ImidazoleHCID 24386Thionyl ChlorideHCID 2793564,4'-DimethylbenzhydrolHCID 67427375HCID 67427375, Verbindung

Produkt 1

HCID 674273871-[Bis(methylphenyl)methyl]imidazole

Versuchsvorschrift

With the same method as for Compound 40, Compound 14 described above, thionyl chloride (Wako Pure Chemical Industries, Ltd.), and imidazole (Wako Pure Chemical Industries, Ltd.) were used, to thereby obtain the title compound.

Quellen und Nachweise

ORD-Eintrag
ord-90d59c0a8fc3457cb4cc696377965feb
Quelldatensatz
uspto-grants-2014_09
Patentnummer
US08846012B2

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