3-Pyridinylboronic acid → 4-(3,3'-Bipyridin-5-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane
Reaktionsgleichung
Br[C:2]1[CH:3]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:5]=[N:6][CH:7]=1.[N:19]1[CH:24]=[CH:23][CH:22]=[C:21](B(O)O)[CH:20]=1>>[N:6]1[CH:5]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:3]=[C:2]([C:21]2[CH:20]=[N:19][CH:24]=[CH:23][CH:22]=2)[CH:7]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared from the product of Example 65A and 3-pyridinylboronic acid according to General Method B: LC-MS Method B (ESI+) m/z 307.0 (M+H)+, retention time 1.54 minutes.
Quellen und Nachweise
- ORD-Eintrag
- ord-74e1ab3e68bf4994a720e0d471debe66
- Quelldatensatz
- uspto-grants-2014_09