HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pyridine → 1-cyclohexyl-3,5-dimethyl-1H-pyrazole-4-carboxylic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pyridine | HCID 1049 | — |
| Edukt | Ethyl 2-acetylacetoacetate | HCID 79063 | — |
| Edukt | Cyclohexylhydrazine hydrochloride | HCID 207836 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-cyclohexyl-3,5-dimethyl-1H-pyrazole-4-carboxylic acid ethyl ester | HCID 9794939 | — |
Reaktionsschritte
Similar to Example 1, equimolar amounts of cyclohexyl hydrazine hydrochloride and 2-acetyl-3-oxobutyric acid ethyl ester were combined in a solution of 50% pyridine in ethanol. Analysis confirmed synthesis of the named product (m.p. 66° C.–67° C.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087634B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-41bda36bf6214c4a9b8efca6708532c2 |
| Quellennotiz | uspto-grants-2006_08 |