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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 8071Erstellt: 24. Oktober 2026

Pyridine → 1-(3-methoxyphenyl)-3,5-dimethyl-1H-pyrazole-4-carboxylic acid ethyl ester

https://huagongshe.com/de/reaction/8071

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktEthyl 2-acetylacetoacetateHCID 79063—
Edukt3-Methoxyphenylhydrazine hydrochlorideHCID 2723940—
LösungsmittelEthanolHCID 702—
Produkt1-(3-methoxyphenyl)-3,5-dimethyl-1H-pyrazole-4-carboxylic acid ethyl esterHCID 9878654—

Reaktionsschritte

Similar to Example 1, equimolar amounts of 3-methoxyphenylhydrazine hydrochloride and 2-acetyl-3-oxo-butyric acid ethyl ester were combined in a solution of 50% pyridine in ethanol. The resulting solid was determined to be the named product by 1H-NMR (CDCl3, ppm): 1.38 t (3H); 2.50 s (3H); 2.52 s (3H); 3.84 s (3H); 4.32 q (2H); 6.96 m (3H); 7.3 st (1H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07087634B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-6d47505205454e4dbf465abd74ce19e3
Quellennotizuspto-grants-2006_08