Hydrochloric Acid → HCID 55285125, Verbindung

Reaktionsgleichung

C(OC(=O)[NH:7][C@@H:8]1[CH2:13][CH2:12][N:11]([CH3:14])[CH2:10][C@H:9]1[O:15][CH3:16])(C)(C)C.Cl>>[CH3:16][O:15][C@H:9]1[C@H:8]([NH2:7])[CH2:13][CH2:12][N:11]([CH3:14])[CH2:10]1

Komponenten

Edukt 2

HCID 313Hydrochloric Acid

HCID 58522509HCID 58522509, Verbindung

Produkt 1

HCID 55285125HCID 55285125, Verbindung

Versuchsvorschrift

Tert-butyl((3R,4R)-3-methoxy-1-methyl-piperidin-4-yl)-carbamate (3.01 g) is combined with HCl (4 molar in dioxane, 25 mL). After 1 h the reaction mixture is freed from the solvent in vacuo and used in the next step without any further purification.

Aufarbeitung

customused in the next step without any further purification

Quellen und Nachweise

ORD-Eintrag: ord-b1c6daa410044df38f2e64041c452c3a
Quelldatensatz: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08846689B2

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