HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 82491Erstellt: 24. Oktober 2026
Trifluoroacetic acid → Amino-acetic acid 4-allyl-2-methoxy-phenyl ester Trifluoroacetate
https://huagongshe.com/de/reaction/82491
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Trifluoroacetic acid | HCID 6422 | — |
| Edukt | Amino-acetic acid 4-allyl-2-methoxy-phenyl ester | HCID 69920127 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Amino-acetic acid 4-allyl-2-methoxy-phenyl ester Trifluoroacetate | HCID 86674925 | — |
Reaktionsschritte
To a solution of compound amino-acetic acid 4-allyl-2-methoxy-phenyl ester (0.3 g) in DCM (10 mL) was added trifluoroacetic acid (0.5 mL) drop wise at (0° C.). The mixture was allowed to stir at room temperature (25° C.) over a period of 2 h. Solvent was stripped off completely and the reaction was carried for the next step (510 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08846721B2 |
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| Quelldatensatz | uspto-grants-2014_09 |
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| ORD ID | ord-94416477fee4402b9dae8b9b83cdb00f |
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| Quellennotiz | uspto-grants-2014_09 |
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