4-Methoxybenzenesulfonyl chloride → 1-[(4-Methoxyphenyl)sulfonyl]-4-(1-piperazinyl)-1H-indole Hydrochloride

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	4-Methoxybenzenesulfonyl chloride	HCID 7401	—
Edukt	tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate	HCID 22015386	—
Produkt	1-[(4-Methoxyphenyl)sulfonyl]-4-(1-piperazinyl)-1H-indole Hydrochloride	HCID 10294853	—

Reaktionsschritte

The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 4-methoxyphenylsulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.07 (br, 1 H), 7.90 (d, J=8 Hz, 2 H), 7.78 (d, J=5 Hz, 1 H), 7.61 (d, J=8 Hz, 1 H), 7.25 (t, J=8 Hz, 1 H), 7.09 (d, J=8 Hz, 2 H), 6.92 (d, J=5 Hz, 1 H), 6.68 (d, J=8 Hz, 1 H), 3.79 (s, 3 H), 3.24 (m, 8 H); MS (ESI+) for m/z 371 (M+H)+.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07087750B2
Quelldatensatz	uspto-grants-2006_08
ORD ID	ord-cf519e59ac3e498dbf8b96e2bf5828fe
Quellennotiz	uspto-grants-2006_08