HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Piperidine → 4-Piperidinylbut-1-ene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Piperidine | HCID 8082 | — |
| Edukt | Homoallyl bromide | HCID 21241 | — |
| Produkt | 4-Piperidinylbut-1-ene | HCID 4562282 | 93,4% |
Reaktionsschritte
4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087757B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-d7ef957ab1cf46f68f1f4c42cdc7ceea |
| Quellennotiz | uspto-grants-2006_08 |