HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → 2-[4-Hydroxyphenyl]-8-methylimidazo[1,2-a]pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 2-Bromo-1-(4-hydroxyphenyl)ethanone | HCID 4964 | — |
| Edukt | 2-Aminopicoline | HCID 66824522 | — |
| Produkt | 2-[4-Hydroxyphenyl]-8-methylimidazo[1,2-a]pyridine | HCID 22015659 | — |
Reaktionsschritte
The product of step A (30 g) and 2-aminopicoline (15 mL) in ethanol (200 mL) was heated at reflux temperature for 4 hours then cooled to ambient temperature. The resulting precipitate containing the title compound was isolated via filtration (27 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087757B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-b69a26f17c554d17b35eebf5deba32e4 |
| Quellennotiz | uspto-grants-2006_08 |