HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
alpha-Methylene-gamma-Butyrolactone Acrylic Acid → alpha-Methylene-gamma-Valerolactone Acrylic Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | alpha-Methylene-gamma-Butyrolactone Acrylic Acid | HCID 86664973 | — |
| Lösungsmittel | Dimethyl Sulfoxide | HCID 679 | — |
| Produkt | alpha-Methylene-gamma-Valerolactone Acrylic Acid | HCID 86664974 | — |
Reaktionsschritte
To a scintillation vial was added 267 mg of the poly(α-methylene-γ-butyrolactone-acrylic acid) prepared in Example 14 and 5.14 mL DMSO on a platform shaker. Once dissolved, the solution was pipetted onto a foil-lined steel panel and placed in a 100° C. oven. Vacuum was applied to remove the solvent over approximately 60 minutes. The result was a 2 cm×2 cm transparent poly(α-methylene-γ-valerolactone-acrylic acid) film.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08846817B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-ffd324aa38484223a081589824c36559 |
| Quellennotiz | uspto-grants-2014_09 |