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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 83943Erstellt: 24. Oktober 2026

alpha-Methylene-gamma-Butyrolactone Acrylic Acid → alpha-Methylene-gamma-Valerolactone Acrylic Acid

https://huagongshe.com/de/reaction/83943

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Eduktalpha-Methylene-gamma-Butyrolactone Acrylic AcidHCID 86664973—
LösungsmittelDimethyl SulfoxideHCID 679—
Produktalpha-Methylene-gamma-Valerolactone Acrylic AcidHCID 86664974—

Reaktionsschritte

To a scintillation vial was added 267 mg of the poly(α-methylene-γ-butyrolactone-acrylic acid) prepared in Example 14 and 5.14 mL DMSO on a platform shaker. Once dissolved, the solution was pipetted onto a foil-lined steel panel and placed in a 100° C. oven. Vacuum was applied to remove the solvent over approximately 60 minutes. The result was a 2 cm×2 cm transparent poly(α-methylene-γ-valerolactone-acrylic acid) film.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08846817B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-ffd324aa38484223a081589824c36559
Quellennotizuspto-grants-2014_09