HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → HCID 20323003, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 9,10-Anthracenedione, 1,4,5,8-tetrachloro- | HCID 66484 | — |
| Edukt | HCID 178418395 | HCID 178418395 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | HCID 20323003 | HCID 20323003 | 90,2% |
Reaktionsschritte
The dyestuff used can be prepared as follows: 15 g of 1,4,5,8-tetrachloro-anthraquinone, 75 g of dimethylformamide, 35 g of 2-mercaptobenzthiazole and 30 g of potassium carbonate are heated to 125°-130° C for about 3 hours. After cooling, the dyestuff which has precipitated in attractive red prisms is filtered off and washed with methanol and water. After drying, 34 g of 1,4,5,8-tetra-(2-benzthiazolyl-thio)-anthraquinone = 90% of theory are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04096111 |
| Quelldatensatz | uspto-grants-1978_06 |
| ORD ID | ord-fffa3eaafbea410f8682c6dc41685fef |
| Quellennotiz | uspto-grants-1978_06 |