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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 839485Erstellt: 25. Oktober 2026

Potassium Carbonate → HCID 20323003, Verbindung

https://huagongshe.com/reaction/839485

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
Edukt9,10-Anthracenedione, 1,4,5,8-tetrachloro-HCID 66484—
EduktHCID 178418395HCID 178418395—
LösungsmittelDimethylformamideHCID 6228—
ProduktHCID 20323003HCID 2032300390,2%

Reaktionsschritte

The dyestuff used can be prepared as follows: 15 g of 1,4,5,8-tetrachloro-anthraquinone, 75 g of dimethylformamide, 35 g of 2-mercaptobenzthiazole and 30 g of potassium carbonate are heated to 125°-130° C for about 3 hours. After cooling, the dyestuff which has precipitated in attractive red prisms is filtered off and washed with methanol and water. After drying, 34 g of 1,4,5,8-tetra-(2-benzthiazolyl-thio)-anthraquinone = 90% of theory are obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04096111
Quelldatensatzuspto-grants-1978_06
ORD IDord-fffa3eaafbea410f8682c6dc41685fef
Quellennotizuspto-grants-1978_06