HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 841152Erstellt: 25. Oktober 2026
Chlorotrimethylsilane → 1-Chloro-3,7-dimethyl-octa-2,6-diene
https://huagongshe.com/reaction/841152
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
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| Edukt | Chlorotrimethylsilane | HCID 6397 | — |
| Edukt | Linalool | HCID 6549 | — |
| Katalysator | Bismuthyl (ion) | HCID 5237718 | — |
| Produkt | 1-Chloro-3,7-dimethyl-octa-2,6-diene | HCID 99106 | 83,2% |
Reaktionsschritte
To a mixture of 170 g linalool and 20 mg bismuth(III)-oxide heated to 60° C., 130.5 g trimethylchlorosilane were dropped in. Then the mixture was cooled to room temperature and the organic layer was separated. The resulting oil was purified by distillation to yield 158.35 g of a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06369248B1 |
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| Quelldatensatz | uspto-grants-2002_04 |
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| ORD ID | ord-93b7fdeaec43433281661a380319a923 |
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| Quellennotiz | uspto-grants-2002_04 |
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