Ammonium Chloride → 2,3,6,7-Tetrahydro-[1,4]oxazepin-5-ylamine monohydrochloride

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Reaktionsgleichung

[O:1]1[CH2:7][CH2:6][C:5](=O)[NH:4][CH2:3][CH2:2]1.[Cl-:9].[NH4+:10]>>[ClH:9].[NH:10]=[C:5]1[CH2:6][CH2:7][O:1][CH2:2][CH2:3][NH:4]1

Komponenten

Edukt 2

HCID 25517Ammonium Chloride

HCID 70230201,4-Oxazepan-5-one

Produkt 1

HCID 226177592,3,6,7-Tetrahydro-[1,4]oxazepin-5-ylamine monohydrochloride

Versuchsvorschrift

Employing the procedure in Example 2, step D, tetrahydro-(2H)-1,4-oxazepin-5-one was reacted with Meerwien's salt and ammonium chloride to form-hexahydro-5-imino-1H-1,4-oxazepine, hydrochloride.

Quellen und Nachweise

ORD-Eintrag: ord-54f9a0e27aa0448d83a0b4e32f7f7641
Quelldatensatz: uspto-grants-2002_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06372733B1

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