Methyl Carbamate → Methyl 2-((2-chlorophenyl)(methyl)carbamoyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepin-8-ylcarbamate

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Methyl Carbamate	HCID 11722	—
Edukt	8-bromo-N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide	HCID 44242427	—
Produkt	Methyl 2-((2-chlorophenyl)(methyl)carbamoyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepin-8-ylcarbamate	HCID 44242426	—

Reaktionsschritte

Following the procedure of Example 61, 8-bromo-N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide 150 and methyl carbamate were coupled to give 149. MS: (ESI+) 443.1

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08846762B2
Quelldatensatz	uspto-grants-2014_09
ORD ID	ord-0bcb1666a17444b89076d1e504df02e6
Quellennotiz	uspto-grants-2014_09