Hydroquinone → Acetic acid, hydroxy((1-oxo-2-propenyl)amino)-, butyl ester

HRID 845873Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 845873
C(N)(=O)C=C.COC.C1(C=CC(O)=CC=1)O.C(N(CC(O)=O)CC(O)=O)CN(CC(O)=O)CC(O)=O.C([O:41][CH:42]([NH:50][C:51](=[O:54])[CH:52]=[CH2:53])[C:43]([O:45][CH2:46][CH2:47][CH2:48][CH3:49])=[O:44])CCC>C(O)CCC>[C:51]([NH:50][CH:42]([OH:41])[C:43]([O:45][CH2:46][CH2:47][CH2:48][CH3:49])=[O:44])(=[O:54])[CH:52]=[CH2:53]

Komponenten

7

Edukt 5

HCID 785HydroquinoneHCID 6049Ethylenediaminetetraacetic AcidHCID 6579AcrylamideHCID 8254Dimethyl EtherHCID 57312822Butyl (acryloylamino)(butoxy)acetate

Produkt 1

HCID 174780Acetic acid, hydroxy((1-oxo-2-propenyl)amino)-, butyl ester

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 2631-ButanolLösungsmittel

Versuchsvorschrift

The procedure of Example I is again followed using the following charge: butyl glyoxylate hemiacetal 315 parts (1.5 moles), acrylamide 110 parts (1.5 moles), methyl ether of hydroquinone 400 parts per million and ethylenediamine tetraacetic acid 200 parts per million. The reaction is run for 3 hours at 60°-65° C. and then by-product butanol is stripped under vacuum. The material is not isolated, instead it is used directly to make butyl acrylamidoglycolate butyl ether.

Aufarbeitung

  1. additionfollowing charge
  2. customThe material is not isolated

Quellen und Nachweise

ORD-Eintrag
ord-e2302c43f63742f8955170b3529b3164
Quelldatensatz
uspto-grants-1988_07
Patentnummer
US04760168

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