HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dibenzylhydroxylamine → N-tert-octyl-[3-(N,N-dibenzylaminoxy)-propionamide]
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dibenzylhydroxylamine | HCID 69297 | — |
| Edukt | N-tert-Octylacrylamide | HCID 171970 | — |
| Edukt | Potassium tert-butoxide | HCID 23665647 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | N-tert-octyl-[3-(N,N-dibenzylaminoxy)-propionamide] | HCID 57149163 | — |
Reaktionsschritte
The procedure of Example I is repeated using 23.31 g of dibenzylhydroxylamine, 1.23 g of potassium-tert-butoxide and 20.0 g of N-tert-octylacrylamide in 100 ml of dry tetrahydrofuran to afford the title compound as a white crystalline solid: mp 96°-98° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04760179 |
| Quelldatensatz | uspto-grants-1988_07 |
| ORD ID | ord-0a1301150065428bb24f377777dcbf8f |
| Quellennotiz | uspto-grants-1988_07 |